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A Gopala Krishna, Dola Sundeep, T Vijaya Kumar (Beteiligte)

Spectroscopic Investigations of MoO3/CuO Nanocomposites


Mechanical Synthesis, Spectroscopic Characterization and Thermal Analysis
2016. 124 S. 220 mm
Verlag/Jahr: SCHOLAR´S PRESS 2016
ISBN: 3-639-86439-5 (3639864395)
Neue ISBN: 978-3-639-86439-7 (9783639864397)

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Nanocomposites extended a wide area of research in Engineering and allied sectors. Molybdenum is an important element used in tribology. For lubrication applications, most of lamellar/layered solid lubricants fail in open air and high temperatures above 773 K, as they turn into oxides. Mixed Oxide such as MoO3- CuO alloy or composite can provide enhanced frictional performance at different high temperatures. In the present book, we synthesized MoO3-CuO composite nanopowders at low cost by mechanical milling and characterized by XRD, SEM with EDS, FT-IR, Raman spectroscopy and TGA/DTA. X-Ray diffraction pattern demonstrates the peaks correspond to orthorhombic phase of _-MoO3 and Monoclinic phase of _-CuO. The average crystalline sizes of the two samples were found to be in 16 and 24nm. Thermogravimetry analysis and Differential Thermal Analysis (DTA) of MoO3-CuO revealed that the dual phase mixed oxide is stable up to 982 K with a negligible weight loss. Hence the synthesized mixed lubricous oxide nanocomposite powders can be used as a solid lubricant at elevated temperatures.
Dola Sundeep Received his graduation in Electronics and CommunicationEngineering in 2013 and Master´s degree in Nanotechnologyin 2015 from Jawaharlal Nehru Technological University Kakinada,India. He is working on nanocomposites and nanoelectronics.